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10.1016/j.jff.2015.06.018 179 ShangY

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Five L of each sample was injected onto a Xbridge amide 3.5 m, 4.6 100 mm column (Waters, Milford, MA) using SIL-30 AC auto sampler (Shimazdu) connected with a high flow LC-30AD solvent delivery unit (Shimazdu) and CBM-20 A communication bus module (Shimazdu) online with QTRAP 5500 (Sciex) operating in positive and negative ion modes